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国家自然科学基金(10979073)

作品数:2 被引量:1H指数:1
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相关机构:中国科学院中国科学院上海应用物理研究所更多>>
发文基金:国家自然科学基金国家重点基础研究发展计划更多>>
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利用同步辐射XRD研究BiFeO_3外延多铁薄膜的微结构被引量:1
2011年
使用脉冲激光沉积在SrTiO3衬底上生长了不同厚度的BiFeO3(BFO)薄膜,X射线衍射分析表明薄膜是BFO外延薄膜.X射线反射率测量发现BFO薄膜密度随着厚度的增加而增加,同时薄膜表面存在厚度为数纳米的非设计覆盖层.随着厚度的增加,BFO薄膜由完全应变过渡到应变部分弛豫状态,同时BFO从四方相转变为单斜相.
李晓龙王灿顾月良何庆吕惠宾金奎娟周兴泰徐洪杰
关键词:铁电薄膜微结构
Quantitative evaluation of equatorial small-angle X-ray scattering for cylindrical fibers
2013年
Elongated microvoids, internal fibrillar structure, and edge scattering from both surface refraction cause an equatorial streak in small angle X-ray scattering. A model for analyzing the edge scattering of fibers is proposed. Simulation results indicate that the intensity of edge scattering from surface refraction of a cylindrical fiber is strong and makes an important contribution to the equatorial streak. Two factors influence edge scattering intensity. One is the sample-to-detector distance (D); edge scattering intensity increases with increasing D. The equatorial streak becomes weak when D is shortened. The other factor is the refraction index. Edge scattering intensity increases as the real component of the refraction index decreases. In experiment, weak or even no equatorial streaks were found for samples measured in a roughly index-matching fluid. Edge scattering can be eliminated or weakened, and it can be calculated by comparing the intensities of a cylindrical fiber when it is measured in air and in index-matching fluid. The simulation data are basically in agreement with the experimental data.
李小芸李秀宏杨春明滑文强赵镍缪夏然田丰王玉柱边风刚王劼
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